石油化工安全环保技术 ›› 2024, Vol. 40 ›› Issue (5): 65-68.

• 清洁生产与综合治理 • 上一篇    

高效液相色谱法同时检测6 种双酚类化合物的方法研究

张哲   

  1. 辽宁省葫芦岛生态环境监测中心,辽宁 葫芦岛 125000
  • 收稿日期:2023-09-07 接受日期:2024-09-15 出版日期:2024-10-20 发布日期:2024-10-30
  • 作者简介:张哲,男,高级工程师,2000 年毕业于辽宁大学环境学专业,现就职于辽宁省葫芦岛生态环境监测中心,任主任助理,电话:13898998868,E-mail :1400450045@qq.com。

Study on Simultaneous Detection of six Bisphenol Compounds by High Performance Liquid Chromatography

Zhang Zhe   

  1. Liaoning Huludao Ecological Environment Monitoring Center, Huludao, Liaoning, 125000
  • Received:2023-09-07 Accepted:2024-09-15 Online:2024-10-20 Published:2024-10-30

摘要: 采用超高效液相色谱法从多种双酚类化合物中选出6 种能同时检测的双酚类化合物,对实验条件进行了优化,确定检出限为0.009~0.012 μg/L,精密度介于0.1%~3.9% 之间,空白加标回收率在80%~114% 之间,为同时检测环境水样中多种双酚类化合物打下良好基础。

关键词: 高效液相色谱法, 多种双酚类化合物, 同时检测

Abstract: In this paper, six bisphenol compounds that could be detected simultaneously were selected from a variety of bisphenol compounds by ultra-performance liquid chromatography. The experimental conditions were optimized and the detection limit was determined to be 0.009 ~ 0.012μg /L; the precision was between 0.1% and 3.9% and the blank spiking recovery was between 80% and 114%. This has laid a good foundation for the simultaneous detection of multiple bisphenol compounds in environmental water samples.

Key words: high performance liquid chromatography (HPLC), multiple bisphenol compounds, simultaneous detection